Standard Test Method for Determination of Lead by Graphite Furnace Atomic Absorption Spectrometry (GFAAS) Techniques

SIGNIFICANCE AND USE
5.1 Environmental (including workplace) samples obtained during the assessment or mitigation of lead hazards from buildings and related structures are analyzed to determine lead content in media of concern. This test method is intended for use with other ASTM standards (see 2.1) that address the collection and preparation of samples (airborne particulate, dusts by wipe and micro-vacuuming, dried paint chips, and soils) that are obtained during the assessment or mitigation of lead hazards. This test method may be used to analyze samples collected from various environments, such as workplaces, buildings, indoor or outdoor settings, construction sites, housing, and so on.  
5.2 This test method may also be used to analyze similar samples from other environments such as toxic characteristic extracts of waste sampled using Guide E1908, and soil and sludge as prepared for analysis using U.S. EPA SW-846 Test Method 1311 (5).  
5.3 This test method can be relied upon by laboratories seeking accreditation for lead analysis by means of GFAAS.
SCOPE
1.1 This test method covers the determination of lead (Pb) in airborne particulate, dust by wipe and micro-vacuuming, paint, and soil collected in and around buildings and related structures using graphite furnace atomic absorption spectrometry (GFAAS).  
1.2 This test method contains directions for sample analysis, as well as quality assurance (QA) and quality control (QC), and may be used for purposes of laboratory accreditation and certification.  
1.3 No detailed operating instructions are provided because of differences among various makes and models of suitable GFAAS instruments. Instead, the analyst shall follow the instructions provided by the manufacturer of the particular instrument.  
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.4.1 Exception—The SI and inch-pound units shown for wipe and micro-vacuuming sampling data are to be individually regarded as standard for wipe and micro-vacuuming sampling data.  
1.5 This test method contains notes which are explanatory and not part of the mandatory requirements of this standard.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
31-Mar-2024
Current Stage
Ref Project

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ASTM D8568-24 - Standard Test Method for Determination of Lead by Graphite Furnace Atomic Absorption Spectrometry (GFAAS) Techniques
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This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D8568 − 24
Standard Test Method for
Determination of Lead by Graphite Furnace Atomic
1
Absorption Spectrometry (GFAAS) Techniques
This standard is issued under the fixed designation D8568; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 2. Referenced Documents
2
1.1 This test method covers the determination of lead (Pb) 2.1 ASTM Standards:
in airborne particulate, dust by wipe and micro-vacuuming, D1193 Specification for Reagent Water
paint, and soil collected in and around buildings and related D1356 Terminology Relating to Sampling and Analysis of
structures using graphite furnace atomic absorption spectrom- Atmospheres
etry (GFAAS). D3919 Practice for Measuring Trace Elements in Water by
Graphite Furnace Atomic Absorption Spectrophotometry
1.2 This test method contains directions for sample analysis,
D4210 Practice for Intralaboratory Quality Control Proce-
as well as quality assurance (QA) and quality control (QC), and
dures and a Discussion on Reporting Low-Level Data
may be used for purposes of laboratory accreditation and
3
(Withdrawn 2002)
certification.
D4532 Test Method for Respirable Dust in Workplace At-
1.3 No detailed operating instructions are provided because
mospheres Using Cyclone Samplers
of differences among various makes and models of suitable
D4697 Guide for Maintaining Test Methods in the User’s
3
GFAAS instruments. Instead, the analyst shall follow the
Laboratory (Withdrawn 2009)
instructions provided by the manufacturer of the particular
D4840 Guide for Sample Chain-of-Custody Procedures
instrument.
D6785 Test Method for Determination of Lead in Workplace
1.4 The values stated in SI units are to be regarded as Air Using Flame or Graphite Furnace Atomic Absorption
Spectrometry
standard. No other units of measurement are included in this
standard. D6966 Practice for Collection of Settled Dust Samples
Using Wipe Sampling Methods for Subsequent Determi-
1.4.1 Exception—The SI and inch-pound units shown for
nation of Metals
wipe and micro-vacuuming sampling data are to be individu-
ally regarded as standard for wipe and micro-vacuuming D7035 Test Method for Determination of Metals and Met-
alloids in Airborne Particulate Matter by Inductively
sampling data.
Coupled Plasma Atomic Emission Spectrometry (ICP-
1.5 This test method contains notes which are explanatory
AES)
and not part of the mandatory requirements of this standard.
D7144 Practice for Collection of Surface Dust by Micro-
1.6 This standard does not purport to address all of the
vacuum Sampling for Subsequent Determination of Met-
safety concerns, if any, associated with its use. It is the
als and Metalloids
responsibility of the user of this standard to establish appro-
D8358 Guide for Assessment and Inclusion of Wall Deposits
priate safety, health, and environmental practices and deter-
in the Analysis of Single-Stage Samplers for Airborne
mine the applicability of regulatory limitations prior to use.
Particulate Matter
1.7 This international standard was developed in accor-
E456 Terminology Relating to Quality and Statistics
dance with internationally recognized principles on standard-
E691 Practice for Conducting an Interlaboratory Study to
ization established in the Decision on Principles for the
Determine the Precision of a Test Method
Development of International Standards, Guides and Recom-
E1188 Practice for Collection and Preservation of Informa-
mendations issued by the World Trade Organization Technical
tion and Physical Items by a Technical Investigator
Barriers to Trade (TBT) Committee.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
1
This test method is under the jurisdiction of ASTM Committee D22 on Air contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Quality and is the direct responsibility of Subcommittee D22.12 on Sampling and Standards volume information, refer to the standard’s Document Summary page on
Analysis of Lead for Exposure and Risk Assessment. the ASTM website.
3
Current edition approved April 1, 2024. Published April 2024. DOI: 10.1520/ The last approved version of this historical standard is referenced on
D8568-24. www.astm.org.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
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